Details
DESCRIPTION:
Catalytic reaction:
Any catalytic liquid-liquid or liquid-gas reaction involving the use of a catalyst placed in basket can be studies in this set-up. Kinetic parameter of a specific reaction can be estimated & parametric studies can be conducted. The set-up consists of a reactor centrally having one spinning basket derived through a variable speed motor. The metered flow of reactant from feed tank is fed to the reactor at the bottom. The set-up can be used as batch wise of as continuous type. Sampling points are provided for analysis. Port connection for gas inlet is provided at the bottom of the reactor.
The present set-up has a facility to interface the system with computer which enables to log the experimental data using computer. The educational software and data-logging package has been developed for unit. The software environment base is of Lab view of NATIONAL INSTRUMENTS, USA. This software is compatible to interfacing unit designed by “Lab Smith. This software package provides a comprehensive educational software environment within which the investigations can be performed. This software is capable to tabulate the sample readings according to the requirement of experiment under study and results obtained can be compared. The real time data acquisition can be done by interfacing the set-up with computer using software. Software allows the user to have control on data logging, printing the stored data, preparing spread sheets in Excel etc.
EXPERIMENTATION:
- To determine the kinetic parameters for a given reaction.
UTILITIES REQUIRED:
- Water Supply.
- Floor Drain.
- Electricity Supply: 1 Phase, 220 V AC, 0.5 kW.
- Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted.
- Computer System : Pentium IV with DVD Drive, Windows XP, MS-Office XP version pre-loaded. One USB slot required in PC for DATA ACQUISITION CARD.
TECHNICAL DETAILS:
Reactor Vessel |
Material Stainless Steel Effective Volume : 1000 ml. |
Basket |
Material Stainless Steel, Fitted with appropriate Stainless Steel. |
Drive for Basket |
DC Motor with Thyristor controlled DC Drive for Variable Speed. |
Packing |
Catalyst |
Feed Tank (1Nos.) |
Material Stainless Steel, Capacity - 10 Ltrs. |
Flow Measurement |
Peristaltic Pumps, 1No. for feed |
Product Analysis |
By using Electronic Sensor, Output 4-20 mA. |
Receiver |
Material Stainless Steel, Capacity 10 Ltrs. |
Piping |
Stainless Steel and PVC. Size ¼” |
Hot water Circulation (in outer Jacket) |
Magnetic Pump of Poly propylene to circulate Hot Water maximum working temp. 85°C |
Hot water tank |
Made of Stainless Steel, Double wall,insulated with Ceramic Wool, Capacity : 10-15 ltrs. |
Heaters |
Nichrome wire heater 750-1000 W approx. |
Control panel comprising of |
PID Controller |
0-200°C (For Hot Water Tank) |
Digital Temp. Indicator |
0-200°C with multi-channel switch. |
Temperature Measurement |
Temp. Transmitter 0-200°C |
RPM Indicator |
Digital, Non-Contact Type. |
With Standard make On/Off switch, Mains Indicator & fuse etc. |
An ENGLISH instruction manual consisting of experimental procedures, block diagram etc. will be provided along with the Apparatus |
The whole set-up is well designed and arranged on a rigid structure painted with industrial PU Paint. |
Ordering Details:
Catalogue No. |
Description |
JICRE-522 |
SPINNING BASKET REACTOR (With Data Logging Facility) |