Details
DESCRIPTION:
Homogeneous reaction:
In an ideal CSTR (i.e. an ideal steady state flow reactor) the contents in reactor are well mixed and have uniform composition throughout. Thus the exit stream has the same composition as the fluid within the reactor. This type of reactor is known as mixed flow reactor. This set-up is used to study a non-catalytic homogeneous second order liquid phase reaction under isothermal condition.
The set up consists of two feed tanks through which two reactants are fed to the reactor. The flow rate can be varied by changing the speed of peristaltic pump. The CSTR is fitted with stirrer for proper mixing. Constant temperature water bath arrangement is provided to conduct the experiment at various temperatures.
The present set-up has a facility to interface the system with computer which enables to log the experimental data using computer. The educational software and data-logging package has been developed for unit. The software environment base is of Lab view of NATIONAL INSTRUMENTS, USA. This software is compatible to interfacing unit designed by “Lab Smith”. This software package provides a comprehensive educational software environment within which the investigations can be performed. This software is capable to tabulate the sample readings according to the requirement of experiment under study and results obtained can be compared. The real time data acquisition can be done by interfacing the set-up with computer using software. Software allows the user to have control on data logging, printing the stored data, preparing spread sheets in Excel etc
EXPERIMENTATION:
- Sponification Reaction study in Isothermal CSTR.
- To determine the Reaction Rate Constant and effect of temperature on it.
UTILITIES REQUIRED:
- Water Supply.
- Floor Drain.
- Electricity Supply : 1 Phase, 220 V AC, 1.5 kW.
- Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted.
- Computer System : Pentium IV with DVD Drive, Windows XP, MS-Office XP version pre-loaded. One USB slot required in PC for DATA ACQUISITION CARD.
TECHNICAL DETAILS:
| Reactor |
Material Stainless Steel, Volume- 2 Ltrs. (Approx.) |
| Water Bath |
Material Stainless Steel, Double wall, insulated with Ceramic Wool. |
| Heater |
Nichrome wire Heater with Control Unit to control heat input. |
| Agitator |
Material Stainless Steel Impeller and shaft coupled with FHP motor with and Control Unit for variable speed (RPM 50-350 approx.) |
| Feed Tank |
Material Stainless Steel (2Nos.), Capacity - 20 Ltrs. |
| Feed Circulation |
By Peristaltic Pump (2Nos.), computer controlled for different RPM |
| Piping |
Stainless Steel and PVC. |
| Product Analysis |
By using Electronic Sensor, Output 4-20 mA. |
| Temp. Measurement |
By temperature transmitter (1No.), (0-200°C) |
| Control panel comprises of |
Standard make on/off switch, Mains Indicator etc. |
| An ENGLISH instruction manual consisting of experimental procedures, block diagram etc. will be provided along with the Apparatus |
| The whole set-up is well designed and arranged on a rigid structure painted with industrial PU Paint. |
Ordering Details:
| Catalogue No. |
Description |
JICRE-1002
|
COMPUTER CONTROLLED - ISOTHERMAL CONTINUOUS
STIRRED TANK REACTOR(With Data Logging Facility)
|