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SUB - BOILING DISTILLATION ASSEMBLY

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SUB - BOILING DISTILLATION ASSEMBLY

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SUB - BOILING DISTILLATION ASSEMBLY

Water Distillation Unit

The Sub Boiling Distillation Assembly is made from electronic grade transparent  fused quartz. Every possible contact of liquid has been avoided with the ground joint connections. The joints on the inlet pipe and  the outlet vessel are so placed that impurities are removed via the outer wall. The method adopted for distillation Surface Evaporation. The evaporation takes place without boiling by  the action heaters. Evaporation is on the surface and the vapours are heaters. Condensed by a cold finger. During this process of evaporation the liquid perfectly calm. The filling of the vessel takes place by means special inlet funnel. The distillation rate/purity could be controlled through a suitable Auto Transformer or Variable Transformer (optional at extra cost).

Sub Boiling Distillation

Type

SBDS (Single Distillation)

SBDD (Double Distillation)

Heating element

Silica/Quartz (Infrared heater)

Silica/Quartz (Infrared heater) 

No. of Stages

SBDS- Single

SBDS- Double

Power

1200 Wattsa

1200 Watts

Power control

Variable transformer PLC

Variable transformer PLC

Safety

Thermal Switch is provided for safety

in absence of acid

Thermal Switch is provided for safety

in absence of acid

Water cooling

Automatic with Solenoid valve

Automatic with Solenoid valve

Material of construction

Electronic grade high purity Quartz, Nylon/Teflon

Electronic grade high purity Quartz, Nylon/Teflon

 

Specifications

The following distillation rates are obtained once steady evaporation has been achieved.

Distillation Rate (g/min)

W(watts)

H2O

HNO3

HCL

H2SO4

200

1.1

1.2

0.8

-

400

2.8

3.3

2.9

-

600

4.4

5.3

4.9

0.3

800

5.8

7.5

7.1

0.8

These results have been achieved using commercial of acid (with impurity concentrations of greater than 100ng/ml) together with desalinized water.

Impurity Concentration (ng/ml)

 

H2O

HNO3

HCL

Al

<0.05

<0.05

0.07

Cd

0.01

0.01

0.01

Cu

0.04

0.25

0.07

Fe

0.32

0.2

0.6

Mg

 

 

0.06

Pb

0.02

<0.05

<0.05

Zn

 

 

0.04

These values were achieved when the apparatus and all the ancillary vessels were treated prior to the distillation with concentrated HNO3 and of course the usual operational procedures for achieving high purity levels were observed.

 The advantages of Sub Boiling Distillation:

  • Very economical for production of ultra-pure acids and solvents from low grade reagent.
  • Save up to 92% of cost of ultra-pure acids.
  • Up to 750 ml. ultra-pure distillate in an hour.
  • Advantages to produce fresh acids/solvents before each analysis there by avoiding storage and contamination.

The Sub Boiling Distillation Assembly is available in 4 models with yield range of 200ml/hour, 500ml/hour, 1000ml/hour & 2000ml/hour. This has been calculated for water.

Ordering Information:

Cat. No.

Description (yield range ml./hr.)

SUB – DS – 01

Sub Boiling Distillation Assembly: Single Distillation 200 ml/hr

SUB – DD – 01

Sub Boiling Distillation Assembly: Double Distillation 500 ml/hr

SUB – DS – 02

Sub Boiling Distillation Assembly: Single Distillation 1000 ml/hr

SUB – DD – 02

Sub Boiling Distillation Assembly: Double Distillation 2000 ml/hr

Description

Details

SUB - BOILING DISTILLATION ASSEMBLY

Water Distillation Unit

The Sub Boiling Distillation Assembly is made from electronic grade transparent  fused quartz. Every possible contact of liquid has been avoided with the ground joint connections. The joints on the inlet pipe and  the outlet vessel are so placed that impurities are removed via the outer wall. The method adopted for distillation Surface Evaporation. The evaporation takes place without boiling by  the action heaters. Evaporation is on the surface and the vapours are heaters. Condensed by a cold finger. During this process of evaporation the liquid perfectly calm. The filling of the vessel takes place by means special inlet funnel. The distillation rate/purity could be controlled through a suitable Auto Transformer or Variable Transformer (optional at extra cost).

Sub Boiling Distillation

Type

SBDS (Single Distillation)

SBDD (Double Distillation)

Heating element

Silica/Quartz (Infrared heater)

Silica/Quartz (Infrared heater) 

No. of Stages

SBDS- Single

SBDS- Double

Power

1200 Wattsa

1200 Watts

Power control

Variable transformer PLC

Variable transformer PLC

Safety

Thermal Switch is provided for safety

in absence of acid

Thermal Switch is provided for safety

in absence of acid

Water cooling

Automatic with Solenoid valve

Automatic with Solenoid valve

Material of construction

Electronic grade high purity Quartz, Nylon/Teflon

Electronic grade high purity Quartz, Nylon/Teflon

 

Specifications

The following distillation rates are obtained once steady evaporation has been achieved.

Distillation Rate (g/min)

W(watts)

H2O

HNO3

HCL

H2SO4

200

1.1

1.2

0.8

-

400

2.8

3.3

2.9

-

600

4.4

5.3

4.9

0.3

800

5.8

7.5

7.1

0.8

These results have been achieved using commercial of acid (with impurity concentrations of greater than 100ng/ml) together with desalinized water.

Impurity Concentration (ng/ml)

 

H2O

HNO3

HCL

Al

<0.05

<0.05

0.07

Cd

0.01

0.01

0.01

Cu

0.04

0.25

0.07

Fe

0.32

0.2

0.6

Mg

 

 

0.06

Pb

0.02

<0.05

<0.05

Zn

 

 

0.04

These values were achieved when the apparatus and all the ancillary vessels were treated prior to the distillation with concentrated HNO3 and of course the usual operational procedures for achieving high purity levels were observed.

 The advantages of Sub Boiling Distillation:

  • Very economical for production of ultra-pure acids and solvents from low grade reagent.
  • Save up to 92% of cost of ultra-pure acids.
  • Up to 750 ml. ultra-pure distillate in an hour.
  • Advantages to produce fresh acids/solvents before each analysis there by avoiding storage and contamination.

The Sub Boiling Distillation Assembly is available in 4 models with yield range of 200ml/hour, 500ml/hour, 1000ml/hour & 2000ml/hour. This has been calculated for water.

Ordering Information:

Cat. No.

Description (yield range ml./hr.)

SUB – DS – 01

Sub Boiling Distillation Assembly: Single Distillation 200 ml/hr

SUB – DD – 01

Sub Boiling Distillation Assembly: Double Distillation 500 ml/hr

SUB – DS – 02

Sub Boiling Distillation Assembly: Single Distillation 1000 ml/hr

SUB – DD – 02

Sub Boiling Distillation Assembly: Double Distillation 2000 ml/hr

Additional Information

Additional Information

Code No
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