Details
DESCRIPTION:
Catalytic Reaction:
The setup consists of catalyst packed column of Stainless Steel. Reactant from a fed tank is fed to the reactor through liquid distributor, fitted at one end of the column. Some part of product is recycled to the reactor using peristaltic pump. Peristaltic Pumps are provided to measure the individual flow of feed & recycled product.. The feed rate and recycle product ratio can be operated by the respective valves of the Peristaltic Pumps. Samples can be taken periodically from the top outlet of reactor at another end. An arrangement is made to carry out the reaction at Isothermal conditions by circulating the hot water in the outer jacket of the packed bed reactor. Special care is taken for proper mixing of feed & recycle product before its entry to the reactor.
EXPERIMENTATION:
- To determine the Reaction Rate Constant.
UTILITIES REQUIRED:
- Water Supply.
- Floor Drain.
- Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted.
TECHNICAL DETAILS:
| Reactor Column |
Material Stainless SteelDiameter 1”, Length: 500mm (approx). |
| Packing |
Catalyst (Fluid Bed Type) |
| Feed Tank (1Nos.) |
Material Stainless Steel, Capacity - 20 Ltrs.. |
| Flow Measurement |
By Peristaltic Pump (2Nos.) |
| Piping |
Stainless Steel and PVC. |
| Hot water tank |
Made of Stainless steel, Double wall, insulated with Ceramic Wool, Capacity: 10-15 ltrs |
| Hot water Circulation (in outer Jacket) |
Magnetic Pump of Poly propylene to circulate Hot Water maximum, working temp. 85°C |
| Heaters |
Nichrome wire |
| Control panel comprising of |
| Digital Temp. Controller |
PID Controller, 0-199.9°C (For Hot Water Tank) With Standard make On/Off switch, Mains Indicator & fuse etc. |
| An ENGLISH instruction manual consisting of experimental procedures, block diagram etc. will be provided along with the Apparatus |
| The whole set-up is well designed and arranged on a rigid structure painted with industrial PU Paint. |
Ordering Details:
| Catalogue No. |
Description |
| JICRE-021C |
RECYCLE BED REACTOR(Peristaltic Pump Feed System) |