Details
DESCRIPTION:
Catalytic Reaction:
Any catalytic liquid-liquid or liquid-gas reaction involving the use of a catalyst placed in basket can be studies in this set-up. Kinetic parameter of a specific reaction can be estimated & parametric studies can be conducted. The set-up consists of a reactor centrally having one spinning basket derived through a variable speed motor. The metered flow of reactant from feed tank is fed to the reactor at the bottom. The set-up can be used as batch wise of as continuous type. Sampling points are provided for analysis. Port connection for gas inlet is provided at the bottom of the reactor.
EXPERIMENTATION:
- To determine the kinetic parameters for a given reaction.
UTILITIES REQUIRED:
- Water Supply.
- Floor Drain.
- Electricity Supply: 1 Phase, 220 V AC, 0.5 kW.
- Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted.
- Computer System : Pentium IV with DVD Drive, Windows XP, MS-Office XP version pre-loaded. One USB slot required in PC for DATA ACQUISITION CARD.
TECHNICAL DETAILS:
| Reactor Vessel |
Material Stainless Steel Effective Volume : 1000 ml. |
| Basket |
Material Stainless Steel, Fitted with appropriate Stainless Steel. |
| Drive for Basket |
DC Motor with Thyristor controlled DC Drive for Variable Speed. |
| Packing |
Catalyst |
| Feed Tank (1Nos.) |
Material Stainless Steel, Capacity - 10 Ltrs. |
| Flow Measurement |
Rotameter |
| Pressure regulator |
Operating Range 0-2 kg/cm² |
| Pressure Gauge |
Bourdon Type 0-2 kg/cm² Standard make. |
| Receiver |
Material Stainless Steel, Capacity 10 Ltrs. |
| Piping |
Stainless Steel and PVC. |
| Hot water Circulation (in outer Jacket) |
Magnetic Pump of Poly propylene to circulate Hot Water maximum working temp. 85°C |
| Hot water tank |
Made of Stainless Steel, Double wall, insulated with Ceramic Wool. Capacity : 10-15 ltrs. |
| Heaters |
Nichrome wire heater 750-1000 W approx. |
| Control panel comprising of |
| Digital Temp. Controller |
0-200°C RTD PT-100 type (For Hot Water Tank) |
| Digital Temp. Indicator |
0-200°C with multi-channel switch. |
| Temperature Sensors |
RTD PT-100 Type |
| RPM Indicator |
Digital, Non-Contact Type. |
| With Standard make On/Off switch, Mains Indicator & fuse etc. |
| An ENGLISH instruction manual consisting of experimental procedures, block diagram etc. will be provided along with the Apparatus |
| The whole set-up is well designed and arranged on a rigid structure painted with industrial PU Paint. |
Ordering Details:
| Catalogue No. |
Description |
| JICRE-022A |
SPINNING BASKET REACTOR(Compressed Air Feed System) |